ORIGINAL ARTICLE
Figure from article: Dynamic Kinetic Modeling of...
 
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Filter cake clean-up remains a challenging operation in drilling, largely owing to the chemical inertness and low solubility of traditional barite-weighting agents. To address this challenge, we investigated the solubility of MicroMax as a high-density alternative to the traditional weighting agents. The experiments focused on kinetic solubility and static filter cake removal efficiency under High-Pressure/High-Temperature (HPHT) conditions (85 °C and 3.45 MPa). The MicroMax formulation achieved a similar macroscopic filter cake thickness of 3.18 mm, while providing reliable wellbore pressure control, yielding a mud density of 15.0 ppg (at a 300 g dosage) compared with that achieved by barite (13.54 ppg, at a 250 g dosage). A pure MicroMax solubility test was conducted to establish the maximum thermodynamic solubility limit of MicroMax in 20 wt.% EDTA-K plus citric acid solution at 11 g/100 mL. During static HPHT removal testing, the traditional barite cake treated with a DTPA-K-based solution exhibited severe kinetic resistance, plateauing at 25%–30% mass removal after 16 h of exposure. By contrast, the MicroMax/EDTA-K solution (basified with KOH and adjusted to pH 5 using citric acid) removed 12 g out of the initial 24.9 g (48%) after 16 h of exposure, which is equivalent to 84% of the theoretical maximum removal capacity. Finally, this study demonstrated that replacing barite with Micro- Max maintains critical drilling fluid properties while fundamentally resolving filter cake removal challenges through highly efficient chelation. Consequently, this MicroMax/EDTA system offers operators a field-ready solution to reduce non-productive rig time and minimize formation damage.
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